Dažu tianeptīnskābes sāļu iegūšana, struktūra un fizikāli-ķīmiskās īpašības
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Latvijas Universitāte
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Dažu tianeptīnskābes sāļu iegūšana, struktūra un fizikāli–ķīmiskas īpašības. Platoņenko A., zinātniskā vadītāja Dr. chem., vadoša pētniece Orola L. Maģistra darbs, 54 lappuses, 33 attēli, 9 tabulas, 40 literatūras avoti. Latviešu valodā.
Darbā tika iegūti tianeptīnskābes tozilāts, dihidrogēnfosfāts un sulfāts. Veikti to polimorfo un pseidopolimorfo formu meklējumi. Ar monokristāla rentgendifraktometrijas metodi noteikta iegūto sāļu struktūra. Struktūras noteikšanai un precizēšanai izmantotas programmas SHELXS un SHELXL. Tianeptīnskābes sāļu struktūra un īpašības salīdzinātas savā starpā.
Synthesis, structure and physicochemical properties of some tianeptine salts. Platoņenko A., supervisor Dr. chem., lead researcher Orola L. Master’s thesis, 54 pages, 33 pictures, 9 tables, 40 literature references. In latvian. Tianeptine tosylate, dihydrogenphosphate and sulfate have been synthesized. Polymorph and pseudopolymorph screening was performed. Salt structure was determined using single crystal X–ray diffractometry. Structure determination and refinement was made using programs SHELXS and SHELXL. Tianeptine salt structures and physicochemical properties were compared with each other.
Synthesis, structure and physicochemical properties of some tianeptine salts. Platoņenko A., supervisor Dr. chem., lead researcher Orola L. Master’s thesis, 54 pages, 33 pictures, 9 tables, 40 literature references. In latvian. Tianeptine tosylate, dihydrogenphosphate and sulfate have been synthesized. Polymorph and pseudopolymorph screening was performed. Salt structure was determined using single crystal X–ray diffractometry. Structure determination and refinement was made using programs SHELXS and SHELXL. Tianeptine salt structures and physicochemical properties were compared with each other.