Hidrolītiski stabilu silanātu kristāliskā struktūra
Loading...
Date
Authors
Advisor
Journal Title
Journal ISSN
Volume Title
Publisher
Latvijas Universitāte
Language
N/A
Abstract
Darbā gaitā ir iegūti 1-[N-(dimetilamonio)metilspirobi(1-sila-2,5-dioksaciklopentān-3-on)āta un tā 4,4-dimetil- atvasinājuma monokristāli. Izmantojot automātisko rentgendifraktometru BRUKER-NONIUS KappaCCD, uzņemti difrakcijas dati no iegūtiem monokristāliem. Atšifrēta un precizēta vielas kristāliskā struktūra. Iegūtie rezultāti salīdzināti ar literatūras datiem, kā arī veikta to interpretācija.
The monocrystals of 1-[N-(dimethylammonio)methylspirobis(1-sila-2,5-dioxacyclopentan-3-one)ate and its 4,4-dimethyl- derivative have been obtained. Difraction data have been detected from the monocrystals using automatic BRUKER-NONIUS KappaCCD X-ray diffractometer. The compounds crystal structures have been solved and refined. The comparision of obtained results was performed with literature date. The interpretation of the results also has been done.
The monocrystals of 1-[N-(dimethylammonio)methylspirobis(1-sila-2,5-dioxacyclopentan-3-one)ate and its 4,4-dimethyl- derivative have been obtained. Difraction data have been detected from the monocrystals using automatic BRUKER-NONIUS KappaCCD X-ray diffractometer. The compounds crystal structures have been solved and refined. The comparision of obtained results was performed with literature date. The interpretation of the results also has been done.